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Hydrothermal processing for increasing the hydroxyl ion concentration in hydroxyl depleted hydroxyapatite

  • Darta Ubele*
  • , Liene Pluduma
  • , Karlis Agris Gross
  • , Arturs Viksna
  • *Corresponding author for this work
  • Riga Technical University

Research output: Chapter in Book/Report/Conference proceedingConference paperResearchpeer-review

4 Citations (Scopus)

Abstract

Thermal spraying is commercially used to produce hydroxyapatite coatings, but the high temperature depletes hydroxyl ions in the structure. To return hydroxyapatite to its original state, it is necessary to restore the hydroxyl ion content in the structure. In this work, the effect of hydrothermal treatment on the hydroxyl ions was investigated in hydroxyapatite powder and thermally sprayed hydroxyapatite coatings. Samples were hydrothermally treated at 200 °C for 24 h and 48 h. Chemical phases were determined by X-ray diffraction, functional groups and hydroxyl ion concentration was examined by Fourier transform infra-red spectroscopy. Results showed that hydrothermal processing of hydroxyapatite coatings at 200 °C for 48 hours produced the greatest increase in the hydroxyl ion concentration by 29%.

Original languageEnglish
Title of host publicationMaterials Science and Applied Chemistry - 58th International Conference of Materials Science and Applied Chemistry, MSAC 2017
EditorsValdis Kokars
PublisherTrans Tech Publications Ltd
Pages42-47
Number of pages6
ISBN (Print)9783035712384
DOIs
Publication statusPublished - 2018
Event58th International Conference of Materials Science and Applied Chemistry, MSAC 2017 - Riga, Latvia
Duration: 20 Oct 201720 Oct 2017

Publication series

NameKey Engineering Materials
Volume762
ISSN (Print)1013-9826
ISSN (Electronic)1662-9795

Conference

Conference58th International Conference of Materials Science and Applied Chemistry, MSAC 2017
Country/TerritoryLatvia
CityRiga
Period20/10/1720/10/17

Keywords

  • Deconvolution
  • Fourier transform infra-red spectroscopy
  • Hydrothermal treatment
  • Hydroxyapatite
  • Hydroxyl ions

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