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Properties of nanosized ferrite powders and sintered materials prepared by the co-precipitation technology, combined with the spray-drying method

  • Ilmars Zalite*
  • , Gundega Heidemane
  • , Eriks Palcevskis
  • , Mikhail Maiorov
  • *Corresponding author for this work
  • Riga Technical University

Research output: Chapter in Book/Report/Conference proceedingConference paperResearchpeer-review

2 Citations (Scopus)

Abstract

Cobalt and nickel ferrites powders are synthesized by the co-precipitation technology, combined with the spray-drying method. The crystallite size, specific surface area (SSA), magnetic properties of synthesized products are investigated. All the synthesized ferrites are nanocrystalline single phase materials with crystallite size of 5-6 nm, the SSA of 80-85 m2/g and the calculated particle size of 13-15 nm. After spray-drying granules of the size up to 10 μm are obtained. After thermal treatment at 550 and 950°C SSA decreases to 40-50 m2/g and 20-22 m2/g, respectively. The saturation magnetization at these temperatures increase from 17 to 40 emu/g for NiFe2O4 and from 51 to 77 emu/g for CoFe2O4. By the pressure-less sintering method the dense material forms at 1100°C for CoFe2O4 and 1200-1300°C for NiFe2O4.

Original languageEnglish
Title of host publicationEngineering Materials and Tribology XXV
EditorsDagnija Loca
PublisherTrans Tech Publications Ltd
Pages295-299
Number of pages5
ISBN (Print)9783035710724
DOIs
Publication statusPublished - 2017
Event25th International Baltic Conference of Engineering Materials and Tribology – BALTMATTRIB - Riga, Latvia
Duration: 3 Nov 20164 Nov 2016

Publication series

NameKey Engineering Materials
Volume721 KEM
ISSN (Print)1013-9826
ISSN (Electronic)1662-9795

Conference

Conference25th International Baltic Conference of Engineering Materials and Tribology – BALTMATTRIB
Country/TerritoryLatvia
CityRiga
Period3/11/164/11/16

Keywords

  • Co-precipitation and spray-drying method
  • CoFeO
  • Nanoparticles
  • NiFeO

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