Abstract
A novel aqueous sol-gel synthesis technique has been refined to prepare heterometallic (Bi1.75Pb0.25)Sr2CaCu 2Ox and (Bi1.8Pb0.33)Sr 1.87CaCu2Ox (Bi-2212) oxides. The formation of Bi-2212 phase depending on synthesis conditions (duration of annealing, stoichiometry of metals) has been estimated. The synthesized products were characterized by powder X-ray diffraction analysis (XRD) and resistivity measurements. It was demonstrated, that the investigated synthesis conditions only slightly influence on the phase purity and superconducting properties of Bi-2212 phase.
| Original language | English |
|---|---|
| Pages (from-to) | 1547-1553 |
| Number of pages | 7 |
| Journal | Polish Journal of Chemistry |
| Volume | 81 |
| Issue number | 9 |
| Publication status | Published - Sept 2007 |
| Externally published | Yes |
Keywords
- Bi-2212
- High-T superconductors
- Sol-gel synthesis
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