Sol-gel synthesis of calcium hydroxyapatite thin films on quartz substrate using dip-coating and spin-coating techniques

Milda Malakauskaite-Petruleviciene; Zivile Stankeviciute; Aldona Beganskiene; Aivaras Kareiva

doi:10.1007/s10971-014-3394-5

Sol-gel synthesis of calcium hydroxyapatite thin films on quartz substrate using dip-coating and spin-coating techniques

Milda Malakauskaite-Petruleviciene
, Zivile Stankeviciute
, Aldona Beganskiene
, Aivaras Kareiva^*

^*Corresponding author for this work

Vilnius University

Research output: Contribution to journal › Article › peer-review

23 Citations (Scopus)

Abstract

Sol-gel synthesis route was suggested to prepare calcium hydroxyapatite (Ca₁₀(PO₄)₆(OH)₂, CHA) thin films on quartz substrates. CHA thin films were obtained using dip-coating and spin-coating techniques by coating the substrates 1, 5, 15 and 30 times. In the sol-gel process, the ethylenediaminetetraacetic acid and 1,2-ethandiol as complexing agents were used. Moreover, triethanolamine and polyvinyl alcohol were used as gel network forming materials. After each coating procedure the films were annealed at 1,000 °C. The results obtained from dip-coating and spin-coating techniques were compared in this study. It was demonstrated, that the formation of calcium hydroxyapatite depends on dipping (or spinning) time and annealing duration.

Original language	English
Pages (from-to)	437-446
Number of pages	10
Journal	Journal of Sol-Gel Science and Technology
Volume	71
Issue number	3
DOIs	https://doi.org/10.1007/s10971-014-3394-5
Publication status	Published - Sept 2014
Externally published	Yes

Keywords

Calcium hydroxyapatite
Dip-coating
Films
Quartz substrate
Sol-gel processing
Spin-coating

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10.1007/s10971-014-3394-5

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title = "Sol-gel synthesis of calcium hydroxyapatite thin films on quartz substrate using dip-coating and spin-coating techniques",

abstract = "Sol-gel synthesis route was suggested to prepare calcium hydroxyapatite (Ca10(PO4)6(OH)2, CHA) thin films on quartz substrates. CHA thin films were obtained using dip-coating and spin-coating techniques by coating the substrates 1, 5, 15 and 30 times. In the sol-gel process, the ethylenediaminetetraacetic acid and 1,2-ethandiol as complexing agents were used. Moreover, triethanolamine and polyvinyl alcohol were used as gel network forming materials. After each coating procedure the films were annealed at 1,000 °C. The results obtained from dip-coating and spin-coating techniques were compared in this study. It was demonstrated, that the formation of calcium hydroxyapatite depends on dipping (or spinning) time and annealing duration.",

keywords = "Calcium hydroxyapatite, Dip-coating, Films, Quartz substrate, Sol-gel processing, Spin-coating",

author = "Milda Malakauskaite-Petruleviciene and Zivile Stankeviciute and Aldona Beganskiene and Aivaras Kareiva",

year = "2014",

month = sep,

doi = "10.1007/s10971-014-3394-5",

language = "English",

volume = "71",

pages = "437--446",

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TY - JOUR

T1 - Sol-gel synthesis of calcium hydroxyapatite thin films on quartz substrate using dip-coating and spin-coating techniques

AU - Malakauskaite-Petruleviciene, Milda

AU - Stankeviciute, Zivile

AU - Beganskiene, Aldona

AU - Kareiva, Aivaras

PY - 2014/9

Y1 - 2014/9

N2 - Sol-gel synthesis route was suggested to prepare calcium hydroxyapatite (Ca10(PO4)6(OH)2, CHA) thin films on quartz substrates. CHA thin films were obtained using dip-coating and spin-coating techniques by coating the substrates 1, 5, 15 and 30 times. In the sol-gel process, the ethylenediaminetetraacetic acid and 1,2-ethandiol as complexing agents were used. Moreover, triethanolamine and polyvinyl alcohol were used as gel network forming materials. After each coating procedure the films were annealed at 1,000 °C. The results obtained from dip-coating and spin-coating techniques were compared in this study. It was demonstrated, that the formation of calcium hydroxyapatite depends on dipping (or spinning) time and annealing duration.

AB - Sol-gel synthesis route was suggested to prepare calcium hydroxyapatite (Ca10(PO4)6(OH)2, CHA) thin films on quartz substrates. CHA thin films were obtained using dip-coating and spin-coating techniques by coating the substrates 1, 5, 15 and 30 times. In the sol-gel process, the ethylenediaminetetraacetic acid and 1,2-ethandiol as complexing agents were used. Moreover, triethanolamine and polyvinyl alcohol were used as gel network forming materials. After each coating procedure the films were annealed at 1,000 °C. The results obtained from dip-coating and spin-coating techniques were compared in this study. It was demonstrated, that the formation of calcium hydroxyapatite depends on dipping (or spinning) time and annealing duration.

KW - Calcium hydroxyapatite

KW - Dip-coating

KW - Films

KW - Quartz substrate

KW - Sol-gel processing

KW - Spin-coating

UR - https://www.scopus.com/pages/publications/84906054682

U2 - 10.1007/s10971-014-3394-5

DO - 10.1007/s10971-014-3394-5

M3 - Article

AN - SCOPUS:84906054682

SN - 0928-0707

VL - 71

SP - 437

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JO - Journal of Sol-Gel Science and Technology

JF - Journal of Sol-Gel Science and Technology

IS - 3

ER -

Sol-gel synthesis of calcium hydroxyapatite thin films on quartz substrate using dip-coating and spin-coating techniques

Abstract

Keywords

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