Synthesis and crystal structure of 4-aminoquinolinium dicitratoborate monohydrate

I. I. Zviedre; S. V. Belyakov; A. G. Tokmakov

Synthesis and crystal structure of 4-aminoquinolinium dicitratoborate monohydrate

I. I. Zviedre^*
, S. V. Belyakov
, A. G. Tokmakov

^*Corresponding author for this work

Riga Technical University
Latvian Institute of Organic Synthesis

Research output: Contribution to journal › Article › peer-review

5 Citations (Scopus)

Abstract

4-Aminoquinolinium dicitratoborate monohydrate [(4-NH₂)C ₉H₆NH][(C₆H₆O₇) ₂B] • H₂O (I) has been synthesized for the first time. Single crystals have been studied by X-ray crystallography. The structural units of crystal I are large complex dicitratoborate anions with a spirane structure, 4-aminoquinolinium cations and crystal water molecules. The crystal packing of I is three-dimensional. Seventeen independent contacts O(N)-H⋯O and N-H⋯O,o' form an intricate system of hydrogen bonds.

Original language	English
Pages (from-to)	275-284
Number of pages	10
Journal	Russian Journal of Inorganic Chemistry
Volume	53
Issue number	2
Publication status	Published - Feb 2008
Externally published	Yes

Cite this

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title = "Synthesis and crystal structure of 4-aminoquinolinium dicitratoborate monohydrate",

abstract = "4-Aminoquinolinium dicitratoborate monohydrate [(4-NH2)C 9H6NH][(C6H6O7) 2B] • H2O (I) has been synthesized for the first time. Single crystals have been studied by X-ray crystallography. The structural units of crystal I are large complex dicitratoborate anions with a spirane structure, 4-aminoquinolinium cations and crystal water molecules. The crystal packing of I is three-dimensional. Seventeen independent contacts O(N)-H⋯O and N-H⋯O,o' form an intricate system of hydrogen bonds.",

author = "Zviedre, \{I. I.\} and Belyakov, \{S. V.\} and Tokmakov, \{A. G.\}",

year = "2008",

month = feb,

language = "English",

volume = "53",

pages = "275--284",

journal = "Russian Journal of Inorganic Chemistry",

issn = "0036-0236",

publisher = "Pleiades Publishing",

number = "2",

}

TY - JOUR

T1 - Synthesis and crystal structure of 4-aminoquinolinium dicitratoborate monohydrate

AU - Zviedre, I. I.

AU - Belyakov, S. V.

AU - Tokmakov, A. G.

PY - 2008/2

Y1 - 2008/2

N2 - 4-Aminoquinolinium dicitratoborate monohydrate [(4-NH2)C 9H6NH][(C6H6O7) 2B] • H2O (I) has been synthesized for the first time. Single crystals have been studied by X-ray crystallography. The structural units of crystal I are large complex dicitratoborate anions with a spirane structure, 4-aminoquinolinium cations and crystal water molecules. The crystal packing of I is three-dimensional. Seventeen independent contacts O(N)-H⋯O and N-H⋯O,o' form an intricate system of hydrogen bonds.

AB - 4-Aminoquinolinium dicitratoborate monohydrate [(4-NH2)C 9H6NH][(C6H6O7) 2B] • H2O (I) has been synthesized for the first time. Single crystals have been studied by X-ray crystallography. The structural units of crystal I are large complex dicitratoborate anions with a spirane structure, 4-aminoquinolinium cations and crystal water molecules. The crystal packing of I is three-dimensional. Seventeen independent contacts O(N)-H⋯O and N-H⋯O,o' form an intricate system of hydrogen bonds.

UR - https://www.scopus.com/pages/publications/40549098131

M3 - Article

AN - SCOPUS:40549098131

SN - 0036-0236

VL - 53

SP - 275

EP - 284

JO - Russian Journal of Inorganic Chemistry

JF - Russian Journal of Inorganic Chemistry

IS - 2

ER -

Synthesis and crystal structure of 4-aminoquinolinium dicitratoborate monohydrate

Abstract

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