The effect of sintering temperature on the structural and magnetic properties of Ni-Mg substituted CoFe2O4 nanoparticles

Rizuan Mohd Rosnan; Zulkafli Othaman; Ali A. Ati; Rosli Hussin; Shadab Dabagh; Samad Zare

doi:10.4028/www.scientific.net/MSF.846.352

The effect of sintering temperature on the structural and magnetic properties of Ni-Mg substituted CoFe₂O₄ nanoparticles

Rizuan Mohd Rosnan^*
, Zulkafli Othaman
, Ali A. Ati
, Rosli Hussin
, Shadab Dabagh
, Samad Zare

^*Corresponding author for this work

Universiti Teknologi Malaysia

Research output: Chapter in Book/Report/Conference proceeding › Conference paper › Research › peer-review

6 Citations (Scopus)

Abstract

This study evaluates the structural and magnetic properties of Ni-Mg substituted Cobalt ferrite samples prepared through the co-precipitation method. The nominal compositions Co_0.5Ni_0.5₋_xMg_x Fe₂O₄ in the range x = 0.1 have been synthesized and then was sintered at temperature at 700 and 1000°C in the furnace for 10 hour with a heating rate of 5°C/min. The prepared nano-ferrites were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM) and vibration sample magnetometer (VSM). XRD confirmed formation of single phase spinel ferrite with average crystalline size in the range of 27–33 nm. The lattice constant (a), cell volume (V) and X-ray density (ρx) are also calculated from XRD data. Lattice constant (a) decreases with an increase of sintering temperature. Further information about the structure and morphology of the nano-ferrites was obtained from FESEM and results are in good agreement with XRD. Saturation magnetization showed increasing trend with sintering temperature from 700 to 1000°C.

Original language	English
Title of host publication	Main Tendencies in Applied Materials Science
Editors	H. Azhan, K. Azman, Nafisah Osman, Oskar Hasdinor Hassan, R. Abd-Shukor, Mohamad Deraman, W. Kong, Z. Aspanut, M.K. Halimah, Rabaah Syahidah Azis, Rabaah Syahidah Azis, M.R. Sahar, S.A. Halim
Publisher	Trans Tech Publications Ltd
Pages	352-357
Number of pages	6
ISBN (Print)	9783038357520
DOIs	https://doi.org/10.4028/www.scientific.net/MSF.846.352
Publication status	Published - 2016
Externally published	Yes
Event	28th Regional Conference on Solid State Science and Technology, RCSSST 2014 - Cameron Highlands, Pahang, Malaysia Duration: 25 Nov 2014 → 27 Nov 2014

Publication series

Name	Materials Science Forum
Volume	846
ISSN (Print)	0255-5476
ISSN (Electronic)	1662-9752

Conference

Conference	28th Regional Conference on Solid State Science and Technology, RCSSST 2014
Country/Territory	Malaysia
City	Cameron Highlands, Pahang
Period	25/11/14 → 27/11/14

Keywords

Co-precipitation
Cobalt ferrite
Ferrites
Magnetic properties
Nanoparticles

Access to Document

10.4028/www.scientific.net/MSF.846.352

Cite this

Rosnan, R. M., Othaman, Z., Ati, A. A., Hussin, R., Dabagh, S., & Zare, S. (2016). The effect of sintering temperature on the structural and magnetic properties of Ni-Mg substituted CoFe₂O₄ nanoparticles. In H. Azhan, K. Azman, N. Osman, O. H. Hassan, R. Abd-Shukor, M. Deraman, W. Kong, Z. Aspanut, M. K. Halimah, R. S. Azis, R. S. Azis, M. R. Sahar, & S. A. Halim (Eds.), Main Tendencies in Applied Materials Science (pp. 352-357). (Materials Science Forum; Vol. 846). Trans Tech Publications Ltd. https://doi.org/10.4028/www.scientific.net/MSF.846.352

Rosnan, Rizuan Mohd ; Othaman, Zulkafli ; Ati, Ali A. et al. / The effect of sintering temperature on the structural and magnetic properties of Ni-Mg substituted CoFe₂O₄ nanoparticles. Main Tendencies in Applied Materials Science. editor / H. Azhan ; K. Azman ; Nafisah Osman ; Oskar Hasdinor Hassan ; R. Abd-Shukor ; Mohamad Deraman ; W. Kong ; Z. Aspanut ; M.K. Halimah ; Rabaah Syahidah Azis ; Rabaah Syahidah Azis ; M.R. Sahar ; S.A. Halim. Trans Tech Publications Ltd, 2016. pp. 352-357 (Materials Science Forum).

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title = "The effect of sintering temperature on the structural and magnetic properties of Ni-Mg substituted CoFe2O4 nanoparticles",

abstract = "This study evaluates the structural and magnetic properties of Ni-Mg substituted Cobalt ferrite samples prepared through the co-precipitation method. The nominal compositions Co0.5Ni0.5−xMgx Fe2O4 in the range x = 0.1 have been synthesized and then was sintered at temperature at 700 and 1000°C in the furnace for 10 hour with a heating rate of 5°C/min. The prepared nano-ferrites were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM) and vibration sample magnetometer (VSM). XRD confirmed formation of single phase spinel ferrite with average crystalline size in the range of 27–33 nm. The lattice constant (a), cell volume (V) and X-ray density (ρx) are also calculated from XRD data. Lattice constant (a) decreases with an increase of sintering temperature. Further information about the structure and morphology of the nano-ferrites was obtained from FESEM and results are in good agreement with XRD. Saturation magnetization showed increasing trend with sintering temperature from 700 to 1000°C.",

keywords = "Co-precipitation, Cobalt ferrite, Ferrites, Magnetic properties, Nanoparticles",

author = "Rosnan, \{Rizuan Mohd\} and Zulkafli Othaman and Ati, \{Ali A.\} and Rosli Hussin and Shadab Dabagh and Samad Zare",

note = "Publisher Copyright: {\textcopyright} 2016 Trans Tech Publications, Switzerland.; 28th Regional Conference on Solid State Science and Technology, RCSSST 2014 ; Conference date: 25-11-2014 Through 27-11-2014",

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Rosnan, RM, Othaman, Z, Ati, AA, Hussin, R, Dabagh, S & Zare, S 2016, The effect of sintering temperature on the structural and magnetic properties of Ni-Mg substituted CoFe₂O₄ nanoparticles. in H Azhan, K Azman, N Osman, OH Hassan, R Abd-Shukor, M Deraman, W Kong, Z Aspanut, MK Halimah, RS Azis, RS Azis, MR Sahar & SA Halim (eds), Main Tendencies in Applied Materials Science. Materials Science Forum, vol. 846, Trans Tech Publications Ltd, pp. 352-357, 28th Regional Conference on Solid State Science and Technology, RCSSST 2014, Cameron Highlands, Pahang, Malaysia, 25/11/14. https://doi.org/10.4028/www.scientific.net/MSF.846.352

The effect of sintering temperature on the structural and magnetic properties of Ni-Mg substituted CoFe₂O₄ nanoparticles. / Rosnan, Rizuan Mohd; Othaman, Zulkafli; Ati, Ali A. et al.
Main Tendencies in Applied Materials Science. ed. / H. Azhan; K. Azman; Nafisah Osman; Oskar Hasdinor Hassan; R. Abd-Shukor; Mohamad Deraman; W. Kong; Z. Aspanut; M.K. Halimah; Rabaah Syahidah Azis; Rabaah Syahidah Azis; M.R. Sahar; S.A. Halim. Trans Tech Publications Ltd, 2016. p. 352-357 (Materials Science Forum; Vol. 846).

Research output: Chapter in Book/Report/Conference proceeding › Conference paper › Research › peer-review

TY - GEN

T1 - The effect of sintering temperature on the structural and magnetic properties of Ni-Mg substituted CoFe2O4 nanoparticles

AU - Rosnan, Rizuan Mohd

AU - Othaman, Zulkafli

AU - Ati, Ali A.

AU - Hussin, Rosli

AU - Dabagh, Shadab

AU - Zare, Samad

PY - 2016

Y1 - 2016

N2 - This study evaluates the structural and magnetic properties of Ni-Mg substituted Cobalt ferrite samples prepared through the co-precipitation method. The nominal compositions Co0.5Ni0.5−xMgx Fe2O4 in the range x = 0.1 have been synthesized and then was sintered at temperature at 700 and 1000°C in the furnace for 10 hour with a heating rate of 5°C/min. The prepared nano-ferrites were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM) and vibration sample magnetometer (VSM). XRD confirmed formation of single phase spinel ferrite with average crystalline size in the range of 27–33 nm. The lattice constant (a), cell volume (V) and X-ray density (ρx) are also calculated from XRD data. Lattice constant (a) decreases with an increase of sintering temperature. Further information about the structure and morphology of the nano-ferrites was obtained from FESEM and results are in good agreement with XRD. Saturation magnetization showed increasing trend with sintering temperature from 700 to 1000°C.

AB - This study evaluates the structural and magnetic properties of Ni-Mg substituted Cobalt ferrite samples prepared through the co-precipitation method. The nominal compositions Co0.5Ni0.5−xMgx Fe2O4 in the range x = 0.1 have been synthesized and then was sintered at temperature at 700 and 1000°C in the furnace for 10 hour with a heating rate of 5°C/min. The prepared nano-ferrites were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM) and vibration sample magnetometer (VSM). XRD confirmed formation of single phase spinel ferrite with average crystalline size in the range of 27–33 nm. The lattice constant (a), cell volume (V) and X-ray density (ρx) are also calculated from XRD data. Lattice constant (a) decreases with an increase of sintering temperature. Further information about the structure and morphology of the nano-ferrites was obtained from FESEM and results are in good agreement with XRD. Saturation magnetization showed increasing trend with sintering temperature from 700 to 1000°C.

KW - Co-precipitation

KW - Cobalt ferrite

KW - Ferrites

KW - Magnetic properties

KW - Nanoparticles

UR - https://www.scopus.com/pages/publications/84964799581

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DO - 10.4028/www.scientific.net/MSF.846.352

M3 - Conference paper

AN - SCOPUS:84964799581

SN - 9783038357520

T3 - Materials Science Forum

SP - 352

EP - 357

BT - Main Tendencies in Applied Materials Science

A2 - Azhan, H.

A2 - Azman, K.

A2 - Osman, Nafisah

A2 - Hassan, Oskar Hasdinor

A2 - Abd-Shukor, R.

A2 - Deraman, Mohamad

A2 - Kong, W.

A2 - Aspanut, Z.

A2 - Halimah, M.K.

A2 - Azis, Rabaah Syahidah

A2 - Sahar, M.R.

A2 - Halim, S.A.

PB - Trans Tech Publications Ltd

T2 - 28th Regional Conference on Solid State Science and Technology, RCSSST 2014

Y2 - 25 November 2014 through 27 November 2014

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Rosnan RM, Othaman Z, Ati AA, Hussin R, Dabagh S, Zare S. The effect of sintering temperature on the structural and magnetic properties of Ni-Mg substituted CoFe₂O₄ nanoparticles. In Azhan H, Azman K, Osman N, Hassan OH, Abd-Shukor R, Deraman M, Kong W, Aspanut Z, Halimah MK, Azis RS, Azis RS, Sahar MR, Halim SA, editors, Main Tendencies in Applied Materials Science. Trans Tech Publications Ltd. 2016. p. 352-357. (Materials Science Forum). doi: 10.4028/www.scientific.net/MSF.846.352